2,3-di-(4'-methoxyphenyl)succinate d'ethyle

Base Information

• Chemical Name: 2,3-di-(4'-methoxyphenyl)succinate d'ethyle
• CAS No.: 125575-31-7
• Molecular Formula: C₂₂H₂₆O₆
• Molecular Weight: 386.445
• Mol file: 125575-31-7.mol

Synonyms:

Chemical Property of 2,3-di-(4'-methoxyphenyl)succinate d'ethyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-di-(4'-methoxyphenyl)succinate d'ethyle

There total 5 articles about 2,3-di-(4'-methoxyphenyl)succinate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

ethyl p-methoxyphenylacetate (14062-18-1) → ethyl 2-hydroxy-2-(4-methoxyphenyl)acetate (36141-66-9) + 2,3-di-(4'-methoxyphenyl)succinate d'ethyle (125575-31-7)

Guidance literature:

With ammonium peroxydisulfate; hydrogen fluoride; triethylamine; In acetonitrile; for 6h; Heating;

Reference yield: 6.0%

ethyl p-methoxyphenylacetate (14062-18-1) → ethyl (p-methoxyphenyl)oxoacetate (40140-16-7) + ethyl fluoro-[4-methoxyphenyl]acetate (24021-11-2) + 2,3-di-(4'-methoxyphenyl)succinate d'ethyle (125575-31-7)

Guidance literature:

With triethylamine tris(hydrogen fluoride); In acetonitrile; at 13 ℃; anodic oxidation;

DOI:10.1016/S0040-4020(01)89079-7

Reference yield:

ethyl p-methoxyphenylacetate (14062-18-1) → meso-2,3-bis-(4-methoxy-phenyl)-succinic acid diethyl ester (125575-31-7)

Guidance literature:

With di-tert-butyl peroxide; at 140 - 150 ℃;

DOI:10.1039/jr9550004229

upstream raw materials:

ethyl p-methoxyphenylacetate

ethyl 2-bromo-2-(4-methoxyphenyl) acetate

Downstream raw materials:

racem.-2,3-bis-(4-hydroxy-phenyl)-succinic acid

racem.-2,3-bis-(4-methoxy-phenyl)-succinic acid