3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide

Base Information

• Chemical Name: 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide
• CAS No.: 127092-08-4
• Molecular Formula: C₅₁H₅₅N₇O₁₁
• Molecular Weight: 942.038

Synonyms:

Chemical Property of 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide

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Technology Process of 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide

There total 4 articles about 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

phenylacetyl bromide (22535-03-1) + virginiamycin S1 (668-72-4,23152-29-6,117603-96-0) → 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-yl)-amide (127092-08-4) + C51H55N7O11 (127092-09-5)

Guidance literature:

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium iodide; In N,N-dimethyl-formamide; for 168h; Yield given;

Reference yield:

Carbonic acid 2-(3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester 2,2,2-trichloro-ethyl ester (127106-17-6) → 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-yl)-amide (127092-08-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / Zn / methanol / 1 h / Heating

2: 1,8-bis(dimethylamino)naphthalene, KI / dimethylformamide / 168 h

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium iodide; zinc; In methanol; N,N-dimethyl-formamide;

Reference yield:

3-(2,4-Dinitro-phenoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-yl)-amide (127092-11-9) → 3-(2-Oxo-2-phenyl-ethoxy)-pyridine-2-carboxylic acid (3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.06,10]hexacos-15-yl)-amide (127092-08-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / thiophenol, triethylamine / CH₂Cl₂ / 0.12 h

2: 1,8-bis(dimethylamino)naphthalene, KI / dimethylformamide / 168 h

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; thiophenol; triethylamine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

phenylacetyl bromide

virginiamycin S₁

Carbonic acid allyl ester 2-(3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester

Carbonic acid 2-(3-benzyl-12-ethyl-4,16-dimethyl-2,5,11,14,18,21,24-heptaoxo-19-phenyl-17-oxa-1,4,10,13,20-pentaaza-tricyclo[20.4.0.0^6,10]hexacos-15-ylcarbamoyl)-pyridin-3-yl ester 2,2,2-trichloro-ethyl ester

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