(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

Base Information

Chemical Name:(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)
CAS No.:216979-79-2
Molecular Formula:C₂₈H₂₆N₂S₂Zn
Molecular Weight:520.05
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

There total 2 articles about (2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: bis(bis(trimethylsilyl)amido)zinc(II)

: 34302-69-7
2,9-dimethyl-1,10-phenanthroline monohydrate

: 100-53-8
phenylmethanethiol

: 216979-79-2
(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

Guidance literature:: In toluene; Zn complex in toluene added slowly with stirring to neo*H2O and ligand in toluene over 2 h; filtered, washed two times (toluene, diethyl ether), elem. anal.;
DOI:10.1002/ejic.200300501

Reference yield: 68.0%

: zinc perchlorate

: 484-11-7
2.9-dimethyl-1,10-phenanthroline

: 100-53-8
phenylmethanethiol

: 216979-79-2
(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

Guidance literature:: With NaOCH₃; In methanol; mixing equimolar amts. of mercaptan and NaOMe, addn. of 0.5 equiv. of Zn-salt, then 0.5 equiv. of ligand, stirring for 1 h; concn. (vac., pptn.), filtration, washing (MeOH), drying (vac.), recrystn. (ethyl acetate); elem. anal.;
DOI:10.1016/S0020-1693(98)00215-1

Reference yield: 99.0%

: 216979-79-2
(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

: 77-78-1
dimethyl sulfate

: 729572-90-1
(2,9-dimethylphenanthroline) zinc benzylmercaptonate methyl sulfate

Guidance literature:: In chloroform; Zn compound and (MeO)2SO2 in CHCl3 stirred for 2 d; reduction on vol. to 20 ml in vac., layered with Et2O, pptn., filtered, washed twice with Et2O; elem. anal.;
DOI:10.1002/ejic.200300501