(2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

Base Information

Chemical Name:(2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate
CAS No.:729572-78-5
Molecular Formula:C₂₂H₂₀N₂S₂Zn
Molecular Weight:441.936
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

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Technology Process of (2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

There total 1 articles about (2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 216979-79-2
(2,9-dimethylphenanthroline) zinc bis(benzylmercaptonate)

: 42254-28-4
disodium p-xylene-α,α'-dithiolate

: 729572-78-5
(2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

: 3492-64-6
sodium benzylmercaptide

Guidance literature:: In d⁽⁴⁾-methanol; in methanol d6; not isolated, detected by NMR;
DOI:10.1002/ejic.200300501

Reference yield: 81.0%

: 729572-78-5
(2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

: 77-78-1
dimethyl sulfate

: (2,9-dimethylphenanthroline) zinc S(o-CH₂C₆H₄CH₂)SCH₃ methyl sulffate

Guidance literature:: In chloroform; Zn complex mixed with 1 equiv. of ligand in CHCl3, stirred for 2 d; layerd with hexane, crystd. for 1 week, filtered, washed (diethyl ether), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200300501

Reference yield: 47.0%

: 729572-78-5
(2,9-dimethylphenanthroline) zinc o-bis(mercaptomethyl)benzoate

: 74-88-4
methyl iodide

: (2,9-dimethylphenanthroline) zinc iodide S(o-CH₂C₆H₄CH₂)SCH₃

Guidance literature:: In chloroform; mixed with 1 equiv. of CH3I in CHCl3, stirred for 1 h; filtered, washed (diethyl ether), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200300501