(η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

Base Information

Chemical Name:(η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm
CAS No.:141292-21-9
Molecular Formula:C₃₃H₃₈ClN₄P₃Pt
Molecular Weight:814.146
Hs Code.:

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Chemical Property of (η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

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Technology Process of (η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

There total 1 articles about (η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108148-24-9
(η2-P(N(CH2CH2)2N)2)Pt(Cl)PPh3

: 2071-20-7
bis-diphenylphosphinomethane

: 141292-21-9,121288-57-1
(η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

Guidance literature:: In tetrahydrofuran; byproducts: P(C6H5)3; N2-atm., stirring (8 h); evapn. (reduced pressure), washing (hexane), dissoln. (THF), slow diffusion of Et2O; elem. anal.;

Reference yield: 96.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 141292-21-9,121288-57-1
(η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

: {(P(NH(CH₂)2N(CH₂)2)2)Pt(Cl)((C₆H₅)2PCH₂P(C₆H₅)2)}⁽²⁺⁾*2BF₄^(1-)={(P(NH(CH₂)2N(CH₂)2)2)Pt(Cl)((C₆H₅)2PCH₂P(C₆H₅)2)}(BF₄)2

Guidance literature:: In tetrahydrofuran; dropwise addn. of the stoich. amt. of 85 % HBF4*O(C2H5)2 to a stirred soln. of the Pt complex in THF under N2, stirring (8 h), pptn.; filtration, washing (THF), drying (vac.); elem. anal.;

Reference yield: 86.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 141292-21-9,121288-57-1
(η2-P(N(CH2CH2)2N)2)Pt(Cl)dppm

: 141292-23-1
{(P(N(CH₂)2N(CH₂)2)2)Pt{Co(CO)3}((C₆H₅)2PCH₂P(C₆H₅)2)}

Guidance literature:: In tetrahydrofuran; dropwise addn. of Na(Co(CO)4) in THF (from Co2(CO)8 and NaOH in THF) to the solid Pt complex under N2, immediate color change to yellow, stirring (1 h); filtration, concg., layering with hexane, crystn.; elem. anal.;