cis-(CO)2(P(OPh)3)2Fe(H)SnCl₃

Base Information

• Chemical Name: cis-(CO)2(P(OPh)3)2Fe(H)SnCl₃
• CAS No.: 129004-91-7
• Molecular Formula: C₃₈H₃₁Cl₃FeO₈P₂Sn
• Molecular Weight: 958.523
• Mol file: 129004-91-7.mol

Synonyms:

Chemical Property of cis-(CO)2(P(OPh)3)2Fe(H)SnCl₃

Chemical Property:

Purity/Quality:

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Technology Process of cis-(CO)2(P(OPh)3)2Fe(H)SnCl₃

There total 1 articles about cis-(CO)2(P(OPh)3)2Fe(H)SnCl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(CO)2(P(OC6H5)3)2FeH2 (72573-42-3) + tin(IV) chloride (7646-78-8) → cis-(CO)2(P(OPh)3)2Fe(H)SnCl3 (129004-91-7)

Guidance literature:

In diethyl ether; byproducts: HCl; (N2); dropwise addn. of SnCl4 to Fe-complex in Et2O (room temp.), react. (2-3 h); filtration, volatile removal, dissolving (toluene), evapn. to dryness, pptn. on addn. of petrol ether/ether in the cold; elem. anal.;

DOI:10.1016/0022-328X(90)85380-H

upstream raw materials:

(CO)2(P(OC₆H₅)3)2FeH₂

tin(IV) chloride