1-Decanone, 1-(4-methoxyphenyl)-

Base Information

• Chemical Name: 1-Decanone, 1-(4-methoxyphenyl)-
• CAS No.: 101741-01-9
• Molecular Formula: C17H26O2
• Molecular Weight: 262.392
• Mol file: 101741-01-9.mol

Synonyms:

Chemical Property of 1-Decanone, 1-(4-methoxyphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Decanone, 1-(4-methoxyphenyl)-

There total 5 articles about 1-Decanone, 1-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-decanoic acid (334-48-5) + methoxybenzene (100-66-3) → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With 18 wt% tungsten oxide supported on titanium dioxide; at 139.84 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.mcat.2019.110410

Reference yield: 92.0%

1-(4-methoxyphenyl)cyclodecan-1-ol → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With 2,3,5-trimethyl-pyridine; [Ir(2-(2,4-difluorophenyl)-5-(trifluoromethyl)pyridine)₂(5,5'-bis(trifluoromethyl)-2,2'-bipyridyl)](PF₆); thiophenol; In dichloromethane; at 20 ℃; Sealed tube; Inert atmosphere; Irradiation;

DOI:10.1021/jacs.6b06517

Reference yield: 81.0%

octanol (111-87-5) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With trifuran-2-yl-phosphane; C₄₈H₃₄F₆N₄O₄Pd₂; lithium hydroxide; In neat (no solvent); at 100 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/acs.organomet.7b00478

upstream raw materials:

methoxybenzene

n-decanoyl chloride

1-decanoic acid

cyclodecanone

Downstream raw materials:

4-decylphenol

1-n-decyl-4-methoxybenzene

isonicotinic acid-[1-(4-methoxy-phenyl)-decylidenehydrazide]

Refernces

• 1、 Mamidala, Ramesh,Samser, Shaikh,Sharma, Nishant,Lourderaj, Upakarasamy,Venkatasubbaiah, Krishnan. "Isolation and Characterization of Regioisomers of Pyrazole-Based Palladacycles and Their Use in α-Alkylation of Ketones Using Alcohols". supporting information. p. 3343 - 3351. Retrieved 2017/09/18.
• 2、 Sarvari, Mona Hosseini,Sharghi, Hashem. "Solvent-free catalytic Friedel - Crafts acylation of aromatic compounds with carboxylic acids by using a novel heterogeneous catalyst system: p-Toluenesulfonic acid/graphite". . p. 2282 - 2287. Retrieved 2007/10/03.