1-(4-Methoxyphenyl)decan-1-one

Base Information

• Chemical Name: 1-(4-Methoxyphenyl)decan-1-one
• CAS No.: 101741-01-9
• Molecular Formula: C17H26O2
• Molecular Weight: 262.392
• DSSTox Substance ID: DTXSID00514596
• Nikkaji Number: J2.092.901D
• Wikidata: Q82375017
• Mol file: 101741-01-9.mol

Synonyms:1-(4-methoxyphenyl)decan-1-one;101741-01-9;1-(4-Methoxy-phenyl)-decan-1-one;DTXSID00514596;AKOS006201377

Chemical Property of 1-(4-Methoxyphenyl)decan-1-one

Chemical Property:

• XLogP3: 5.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 10
• Exact Mass: 262.193280068
• Heavy Atom Count: 19
• Complexity: 229

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCC(=O)C1=CC=C(C=C1)OC

Technology Process of 1-(4-Methoxyphenyl)decan-1-one

There total 5 articles about 1-(4-Methoxyphenyl)decan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-decanoic acid (334-48-5) + methoxybenzene (100-66-3) → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With 18 wt% tungsten oxide supported on titanium dioxide; at 139.84 ℃; for 6h; Inert atmosphere;

DOI:10.1016/j.mcat.2019.110410

Reference yield: 92.0%

1-(4-methoxyphenyl)cyclodecan-1-ol → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With 2,3,5-trimethyl-pyridine; [Ir(2-(2,4-difluorophenyl)-5-(trifluoromethyl)pyridine)₂(5,5'-bis(trifluoromethyl)-2,2'-bipyridyl)](PF₆); thiophenol; In dichloromethane; at 20 ℃; Sealed tube; Inert atmosphere; Irradiation;

DOI:10.1021/jacs.6b06517

Reference yield: 81.0%

octanol (111-87-5) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 1-(4-methoxyphenyl)decan-1-one (101741-01-9)

Guidance literature:

With trifuran-2-yl-phosphane; C₄₈H₃₄F₆N₄O₄Pd₂; lithium hydroxide; In neat (no solvent); at 100 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/acs.organomet.7b00478

upstream raw materials:

methoxybenzene

n-decanoyl chloride

1-decanoic acid

cyclodecanone

Downstream raw materials:

isonicotinic acid-[1-(4-methoxy-phenyl)-decylidenehydrazide]

1-n-decyl-4-methoxybenzene

4-decylphenol