Technology Process of C11H16O
There total 5 articles about C11H16O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diisobutylaluminium hydride / dichloromethane / -78 °C
2: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C
3: sodium tetrahydroborate / methanol / 0.5 h / 0 °C
4: hydrogen / water; ethanol / 3 h / 760.05 Torr
With
sodium tetrahydroborate; hydrogen; diisobutylaluminium hydride; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride;
In
methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1002/adsc.201300250
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C
2: sodium tetrahydroborate / methanol / 0.5 h / 0 °C
3: hydrogen / water; ethanol / 3 h / 760.05 Torr
With
sodium tetrahydroborate; hydrogen; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride;
In
methanol; ethanol; water; acetonitrile;
DOI:10.1002/adsc.201300250