Plumbanecarbonitrile, triphenyl-

Base Information

Chemical Name:Plumbanecarbonitrile, triphenyl-
CAS No.:10177-50-1
Molecular Formula:C₁₉H₁₅NPb
Molecular Weight:464.535
Hs Code.:
Mol file:10177-50-1.mol

Synonyms:

Suppliers and Price of Plumbanecarbonitrile, triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Plumbanecarbonitrile, triphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Plumbanecarbonitrile, triphenyl-

There total 2 articles about Plumbanecarbonitrile, triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 506-78-5
cyanogen iodide

: 3124-01-4
hexaphenyl diplumbane

: 10177-50-1
triphenyllead cyanide

: 894-07-5
triphenyllead iodide

Guidance literature:: In tetrachloromethane; dropwise addn. of CNI in CCl4 to stirred suspension of Pb2(C6H5)6 in CCl4 during 30 min at room temp.; refluxing for 30 min;; filtration, washing with ether, recrystn. from abs. alcohol yielded Pb(C6H5)3CN; concentrating filtrate and cooling yielded Pb(C6H5)3I; m.p.; IR spectroscopy;;
DOI:10.1016/S0277-5387(00)84419-8

Reference yield: 42.0%

: 506-68-3
bromocyane

: 3124-01-4
hexaphenyl diplumbane

: 10177-50-1
triphenyllead cyanide

: 894-06-4
triphenyl lead bromide

Guidance literature:: In tetrachloromethane; dropwise addn. of CNBr in CCl4 to stirred suspension of Pb2(C6H5)6 in CCl4 during at room temp.; refluxing; reaction time 2 h;; fractional crystn.; repeated recrystn.; m.p.;;
DOI:10.1016/S0277-5387(00)84419-8