iodo(triphenyl)plumbane

Base Information

Chemical Name:iodo(triphenyl)plumbane
CAS No.:894-07-5
Molecular Formula:C₁₈H₁₅IPb
Molecular Weight:565.422
Hs Code.:

Synonyms:

Suppliers and Price of iodo(triphenyl)plumbane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of iodo(triphenyl)plumbane

Chemical Property:

Vapor Pressure:2.28E-08mmHg at 25°C
Boiling Point:464.7°C at 760 mmHg
Flash Point:234.8°C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of iodo(triphenyl)plumbane

There total 4 articles about iodo(triphenyl)plumbane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 3607-48-5
iodine isocyanate

: 3124-01-4
hexaphenyl diplumbane

: 894-07-5
triphenyllead iodide

: triphenyllead isocyanide

Guidance literature:: In tetrachloromethane; dropwise addn. of Pb2(C6H5)6 in CCl4 to stirred soln. of INCO in CCl4 over a period of 15 min at -10°C; stirring at -10°C for 1 h; allowing to reach room temp.;; filtration; fractional crystn. on cooling; repeated recrystn.; m.p.; elem. anal.;;
DOI:10.1016/S0277-5387(00)84419-8

Reference yield: 54.0%

: 506-78-5
cyanogen iodide

: 3124-01-4
hexaphenyl diplumbane

: 10177-50-1
triphenyllead cyanide

: 894-07-5
triphenyllead iodide

Guidance literature:: In tetrachloromethane; dropwise addn. of CNI in CCl4 to stirred suspension of Pb2(C6H5)6 in CCl4 during 30 min at room temp.; refluxing for 30 min;; filtration, washing with ether, recrystn. from abs. alcohol yielded Pb(C6H5)3CN; concentrating filtrate and cooling yielded Pb(C6H5)3I; m.p.; IR spectroscopy;;
DOI:10.1016/S0277-5387(00)84419-8

Reference yield: 48.0%

: 14696-82-3
iodine(I) azide

: 3124-01-4
hexaphenyl diplumbane

: 14127-50-5
triphenyllead azide

: 894-07-5
triphenyllead iodide

Guidance literature:: In tetrachloromethane; dropwise addn. of Pb2(C6H5)6 in CCl4 to stirred soln. of IN3 in CCl4 over a period of 15 min at -10°C; stirring at -10°C for 1 h; allowing to reach room temp.;; filtration; fractional crystn. on cooling; repeated recrystn.; m.p.; IR spectroscopy;;
DOI:10.1016/S0277-5387(00)84419-8