(1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

Base Information

Chemical Name:(1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate
CAS No.:160238-70-0
Molecular Formula:C₂₃H₂₈O₅
Molecular Weight:384.472
Hs Code.:

Synonyms:

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Chemical Property of (1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

Chemical Property:

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Technology Process of (1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

There total 11 articles about (1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 183947-33-3
Benzoic acid (1R,2S,3R)-3-benzyloxy-4-[1,3]dithian-2-yl-1-isopropyl-2-methoxy-butyl ester

: 160238-70-0
(1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

Guidance literature:: With N-Bromosuccinimide; water; In acetone; at -23 ℃; for 0.166667h; Yield given;
DOI:10.1016/0040-4020(96)00811-3

Reference yield:

: 100-39-0
benzyl bromide

: 160238-70-0
(1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / NaH / tetrahydrofuran; dimethylformamide / 12 h / Ambient temperature

2: 81 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

3: DMAP, pyridine / CH₂Cl₂ / 72 h / Ambient temperature

4: NBS, H₂O / acetone / 0.17 h / -23 °C

With pyridine; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0040-4020(96)00811-3

Reference yield:

: 160238-68-6
(2R,3S,4R,6S)-4-benzyloxy-2-isopropyl-3,6-dimethoxy-3,4,5,6-tetrahydro-2H-pyran

: 160238-70-0
(1R,2S,3R)-3-benzyloxy-4-formyl-1-isopropyl-2-methoxybutyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / BF₃*Et₂O / CH₂Cl₂ / 24 h / Ambient temperature

2: DMAP, pyridine / CH₂Cl₂ / 72 h / Ambient temperature

3: NBS, H₂O / acetone / 0.17 h / -23 °C

With pyridine; dmap; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; In dichloromethane; acetone;
DOI:10.1016/0040-4020(96)00811-3