<(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl

Base Information

• Chemical Name: <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl
• CAS No.: 70741-30-9
• Molecular Formula: C₂₄H₃₃N₂O₂S
• Molecular Weight: 413.604
• Mol file: 70741-30-9.mol

Synonyms:

Chemical Property of <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl

There total 4 articles about <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

N-<(4-nitrophenyl)thio>-2,4,6-tri-tert-butylaniline (70741-37-6) → <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl (70741-30-9)

Guidance literature:

With potassium carbonate; lead dioxide; In benzene; for 0.166667h;

Reference yield:

4-nitrobenzenesulfenyl chloride (937-32-6) → <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl (70741-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / triethylamine / diethyl ether / 5 h / Ambient temperature

2: 1.) K₂CO₃, 2.) PbO₂ / 1.) benzene, 10 min

With potassium carbonate; lead dioxide; triethylamine; In diethyl ether;

DOI:10.1021/jo00134a020

Reference yield:

2,4,6-Tri-tert-butylaniline (961-38-6) → <(4-nitrophenyl)thio>(2,4,6-tri-tert-butylphenyl)aminyl (70741-30-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / triethylamine / diethyl ether / 5 h / Ambient temperature

2: 1.) K₂CO₃, 2.) PbO₂ / 1.) benzene, 10 min

With potassium carbonate; lead dioxide; triethylamine; In diethyl ether;

DOI:10.1021/jo00134a020

upstream raw materials:

N-<(4-nitrophenyl)thio>-2,4,6-tri-tert-butylaniline

4-nitrobenzenesulfenyl chloride

2,4,6-Tri-tert-butylaniline