Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

Base Information

Chemical Name:Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester
CAS No.:125031-05-2
Molecular Formula:C₃₃H₂₂ClN₅O₃S
Molecular Weight:604.088
Hs Code.:

Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

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Chemical Property of Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

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Technology Process of Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

There total 6 articles about Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67860-46-2
5-(2-chlorophenyl)-2-hydrazino-7-iodo-3H-thieno<2,3-e><1,4>diazepine

: 125031-05-2
Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 74.5 percent / p-TSA / ethyl acetate / 0.5 h / Heating

2: 76 percent / PPh₃, CuI, Et₃N, palladium acetate / dimethylformamide / 72 h / Ambient temperature

3: 79 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

4: pyridine / 4 h / Heating

With pyridine; copper(l) iodide; palladium diacetate; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00107a048

Reference yield:

: 67860-41-7
4-(2-chlorophenyl)2-iodo-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepine

: 125031-05-2
Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / PPh₃, CuI, Et₃N, palladium acetate / dimethylformamide / 72 h / Ambient temperature

2: 79 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

3: pyridine / 4 h / Heating

With pyridine; copper(l) iodide; palladium diacetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00107a048

Reference yield:

: 125030-71-9
5-{3-[4-(2-chlorophenyl)-9-methyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-2-yl]-2-propynyl}-phenanthridin-6(5H)-one

: 125031-05-2
Acetic acid 4-(2-chloro-phenyl)-9-methyl-2-[3-(6-oxo-6H-phenanthridin-5-yl)-prop-1-ynyl]-6H-1-thia-5,7,8,9a-tetraaza-cyclopenta[e]azulen-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

2: pyridine / 4 h / Heating

With pyridine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00107a048