C₄₈H₃₇FeN₄O₄S

Base Information

Chemical Name:C₄₈H₃₇FeN₄O₄S
CAS No.:92763-27-4
Molecular Formula:C₄₈H₃₇FeN₄O₄S
Molecular Weight:821.759
Hs Code.:

C<sub>48</sub>H<sub>37</sub>FeN<sub>4</sub>O<sub>4</sub>S

Synonyms:

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Chemical Property of C₄₈H₃₇FeN₄O₄S

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Technology Process of C₄₈H₃₇FeN₄O₄S

There total 2 articles about C₄₈H₃₇FeN₄O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 333460-15-4,36995-20-7
(5,10,15,20-tetrakis(4-methoxyphenyl)-21H,23H-porphine)iron(III) chloride

: 92763-27-4
C₄₈H₃₇FeN₄O₄S

: 57715-41-0
5,10,15,20-tetrakis(4-methoxylphenyl)porphyrinate iron(II)

Guidance literature:: With sulfur; LiBEt₃H; In tetrahydrofuran; 1,1,2-trichloroethane; a soln. prepd. from 1 equiv of sulfur and 2 equiv of LiBEt3H (containing primarily Li2S) was added to Fe(III)-complex in dry CHCl2CH2Cl under N2; no hydrosulfido Fe(III)-complex was formed;
DOI:10.1021/ja00335a074

Reference yield:

: 10544-50-0
sulfur

: 333460-15-4,36995-20-7
(5,10,15,20-tetrakis(4-methoxyphenyl)-21H,23H-porphine)iron(III) chloride

: 92763-27-4
C₄₈H₃₇FeN₄O₄S

: μ-sulfidobis{{5,10,15,20-tetrakis(p-methoxyphenyl)porphyrinato}iron(III)}

Guidance literature:: With LiB(C₂H₅)3H; In tetrahydrofuran; 1,1,2-trichloroethane; an excess of a soln. containing Li2S (prepd. from 1 equiv of sulfur and 2 equiv of LiBEt3H in THF) was added to Fe(porphyrinato)Cl in dry CHCl2CH2Cl under N2; no bridged sulfide complex was observed; the solvent was immediately pulled off in vacuo at room temp., the residue taken into an inert atmosphere box, dissolved in CH2Cl2, filtered through a plug of Celite, filtrate was concd. with concominant addn. of hexane, crystals were dried in vacuo;
DOI:10.1021/ja00335a074