(C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl

Base Information

• Chemical Name: (C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl
• CAS No.: 333460-15-4
• Molecular Formula: C₄₈H₃₆ClFeN₄O₄
• Molecular Weight: 824.138
• Mol file: 333460-15-4.mol

Synonyms:

Chemical Property of (C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl

There total 8 articles about (C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.2%

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin (22112-78-3) → (5,10,15,20-tetrakis(4-methoxyphenyl)-21H,23H-porphine)iron(III) chloride (333460-15-4,36995-20-7)

Guidance literature:

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin; With iron(II) chloride tetrahydrate; In N,N-dimethyl-formamide; for 0.5h;

With hydrogenchloride; In water; at 50 - 60 ℃;

DOI:10.3390/molecules16042960

Reference yield: 95.2%

iron(II) chloride tetrahydrate + 5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin (22112-78-3) → (5,10,15,20-tetrakis(4-methoxyphenyl)-21H,23H-porphine)iron(III) chloride (333460-15-4,36995-20-7)

Guidance literature:

In N,N-dimethyl-formamide; for 0.5h; Reflux;

DOI:10.1021/op060056z

Reference yield: 90.0%

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin (22112-78-3) + iron(II) chloride → (5,10,15,20-tetrakis(4-methoxyphenyl)-21H,23H-porphine)iron(III) chloride (333460-15-4,36995-20-7)

Guidance literature:

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin; iron(II) chloride; In tetrahydrofuran; for 20h; Reflux; Inert atmosphere; Darkness;

With air; In tetrahydrofuran; at 20 ℃; for 0.333333h; Darkness;

DOI:10.1016/j.tet.2016.01.013

upstream raw materials:

iron(III) chloride

{(p-OMeTPP)Fe}2O

pyrrole

4-methoxy-benzaldehyde

Downstream raw materials:

(4Z,9Z,15Z)-5,10,15-tri(4-methoxyphenyl)-(21H,23H,24H)-1,19,21,24-tetrahydro-1,19-bilindione

(4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one

(μ-oxo)bis[(meso-tetrakis(4-methoxyphenyl)porphinato)iron(III)]

C₄₈H₃₇FeN₄O₄S