2-(phenyl methyl)-2,3-dihydrothiopyrane

Base Information

Chemical Name:2-(phenyl methyl)-2,3-dihydrothiopyrane
CAS No.:144617-28-7
Molecular Formula:C₁₂H₁₄S
Molecular Weight:190.309
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(phenyl methyl)-2,3-dihydrothiopyrane

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Technology Process of 2-(phenyl methyl)-2,3-dihydrothiopyrane

There total 3 articles about 2-(phenyl methyl)-2,3-dihydrothiopyrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13042-80-3
3,4-dihydro-2H-thiopyran

: 144617-28-7
2-(phenyl methyl)-2,3-dihydrothiopyrane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / HCl (gas) / diethyl ether / 0.5 h / Ambient temperature

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 2.) THF, hexane, a) RT, 1 h, b) reflux, 1 h

With hydrogenchloride; n-butyllithium; In diethyl ether;