Technology Process of C21H23NO4
There total 3 articles about C21H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper (I) trifluoromethane sulfonate toluene complex;
In
dichloromethane;
Inert atmosphere;
DOI:10.1002/chem.201102583
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: copper (I) trifluoromethane sulfonate toluene complex / dichloromethane / Inert atmosphere
With
copper (I) trifluoromethane sulfonate toluene complex; sodium hydride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201102583
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine; hydroquinone / toluene / 1 h / 85 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: copper (I) trifluoromethane sulfonate toluene complex / dichloromethane / Inert atmosphere
With
pyridine; copper (I) trifluoromethane sulfonate toluene complex; sodium hydride; hydroquinone;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/chem.201102583