2-Methyl-1,3,5-triphenyl-1,5-pentanedione

Base Information

• Chemical Name: 2-Methyl-1,3,5-triphenyl-1,5-pentanedione
• CAS No.: 10226-00-3
• Molecular Formula: C24H22O2
• Molecular Weight: 342.43000
• European Community (EC) Number: 651-792-5
• Nikkaji Number: J536.159A
• Mol file: 10226-00-3.mol

Synonyms:2-methyl-1,3,5-triphenyl-1,5-pentanedione;AKOS024322266;1,3,5-Triphenyl-2-methyl-1,5-pentanedione

Chemical Property of 2-Methyl-1,3,5-triphenyl-1,5-pentanedione

Chemical Property:

• PSA: 34.14000
• LogP: 5.56220
• XLogP3: 5.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 7
• Exact Mass: 342.161979940
• Heavy Atom Count: 26
• Complexity: 451

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-METHYL-1,3,5-TRIPHENYL-1,5-PENTANEDIONE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(CC(=O)C1=CC=CC=C1)C2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of 2-Methyl-1,3,5-triphenyl-1,5-pentanedione

There total 5 articles about 2-Methyl-1,3,5-triphenyl-1,5-pentanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane (66323-99-7) + 1,3-diphenyl-propen-3-one (614-47-1) → 2-methyl-1,3,5-triphenyl-pentane-1,5-dione (10226-00-3)

Guidance literature:

trimethyl[(Z)-(1-phenyl-1-propenyl)oxy]silane; 1,3-diphenyl-propen-3-one; lithium acetate; In N,N-dimethyl-formamide; at 20 ℃; for 10h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1246/cl.2004.1016

Reference yield:

benzalacetophenone (94-41-7) + 1-phenyl-propan-1-one (93-55-0) → 2-methyl-1,3,5-triphenyl-pentane-1,5-dione (10226-00-3)

Guidance literature:

With sodium ethanolate;

Reference yield:

phenylmagnesium bromide + 5-methyl-6-phenyl-(2H)-pyran-2-one (22582-40-7) → 2-methyl-1,3,5-triphenyl-pentane-1,5-dione (10226-00-3)

Guidance literature:

upstream raw materials:

sodium ethanolate

benzalacetophenone

1-phenyl-propan-1-one

5-methyl-6-phenyl-(2H)-pyran-2-one

Downstream raw materials:

3-methyl-2,4,6-triphenyl-pyridine

2-Chloro-4-methyl-1,3,5-triphenyl-pentane-1,5-dione

2,4,6-triphenyl-3-methyl-4H-pyran