dibenzylamine borane

Base Information

Chemical Name:dibenzylamine borane
CAS No.:55124-36-2
Molecular Formula:C₁₄H₁₈BN
Molecular Weight:211.115
Hs Code.:

Synonyms:

Suppliers and Price of dibenzylamine borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzylamine borane

Chemical Property:

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Technology Process of dibenzylamine borane

There total 4 articles about dibenzylamine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19287-45-7
diborane

: 103-49-1
dibenzylamine

: 55124-36-2
dibenzylamine borane

Guidance literature:: In benzene; preparation of B2H6 from NaBH4 and (C2H5)2O*BF3; in diglyme, introduction into a benzene-soln. of the amine; removal of solvent;;

Reference yield:

: 4856-92-2
benzylamine BH₃ adduct

: 100-44-7
benzyl chloride

: 55124-36-2
dibenzylamine borane

Guidance literature:: With s-butyllithium; In tetrahydrofuran; cyclohexane; (N2); dropwise addn. of a soln. of lithium compd. in cyclohexane to a soln. of boron compd. in THF at -78°C, stirring for 30 min, warmingto room temp. for 30 min, addn. of benzyl chloride, stirring overnight at room temp.; not purified;
DOI:10.1016/j.jorganchem.2005.01.059

Reference yield:

: borane tetrahydrofuran

: 103-49-1
dibenzylamine

: 55124-36-2
dibenzylamine borane

Guidance literature:: In tetrahydrofuran; dropwise addn. of 2.0M BH3*THF to a THF soln. of the amine (10 mmol); performed under a dry N2 atm.;; removal of solvent and excess of BH3*THF under reduced pressure immediately after addn.;;
DOI:10.1016/S0277-5387(00)84849-4