Technology Process of 2-(4-Propylphenyl)propane-1,3-diol
There total 5 articles about 2-(4-Propylphenyl)propane-1,3-diol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
diethyl ether;
for 15h;
Ambient temperature;
- Guidance literature:
-
With
sodium tetrahydroborate;
In
ethanol;
at 55 ℃;
DOI:10.1039/b210765a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: concd. hydrochloric acid, calcium chloride / benzene / 1.) room temperature, 3 h, 2.) 55 deg C, 2 h, 3.) reflux, 5 h
2: 1.) LiAlH4, 2.) 5percent sodium hydroxide / 1.) diethyl ether, reflux, 6 h, 2.) ethyl acetate, room temperature, 10 h
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; calcium chloride;
In
benzene;
DOI:10.1246/bcsj.62.3896
