Diethyl-(4-propylphenyl)malonat

Base Information

Chemical Name:Diethyl-(4-propylphenyl)malonat
CAS No.:3585-46-4
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:Diethyl-(4-propylphenyl)malonat

Suppliers and Price of Diethyl-(4-propylphenyl)malonat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diethyl-(4-propylphenyl)malonat

Chemical Property:

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Technology Process of Diethyl-(4-propylphenyl)malonat

There total 4 articles about Diethyl-(4-propylphenyl)malonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 126261-84-5
1-iodo-4-n-propylbenzene

: 105-53-3
diethyl malonate

: 3585-46-4
Diethyl-(4-propylphenyl)malonat

Guidance literature:: With 2-Picolinic acid; copper(l) iodide; caesium carbonate; In tetrahydrofuran; at 70 ℃; for 6h; Inert atmosphere;

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 3585-46-4
Diethyl-(4-propylphenyl)malonat

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium t-butoxide / 2.) dichlorobis(triphenylphosphine)palladium / 1.) 1,2-dimethoxyethane, room temperature, 10 min, 2.) 1,2-dimethoxyethane, 70 deg C, 8 h

2: concd. hydrochloric acid, calcium chloride / benzene / 1.) room temperature, 3 h, 2.) 55 deg C, 2 h, 3.) reflux, 5 h

With hydrogenchloride; potassium tert-butylate; calcium chloride; bis-triphenylphosphine-palladium(II) chloride; In benzene;
DOI:10.1246/bcsj.62.3896

Reference yield:

: 64-17-5
ethanol

: ethyl 4-propylphenylcyanoacetate

: 3585-46-4
Diethyl-(4-propylphenyl)malonat

Guidance literature:: With hydrogenchloride; calcium chloride; In benzene; 1.) room temperature, 3 h, 2.) 55 deg C, 2 h, 3.) reflux, 5 h;
DOI:10.1246/bcsj.62.3896