[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

Base Information

Chemical Name:[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]
CAS No.:1187882-78-5
Molecular Formula:C₁₆H₇BiF₁₂O₄
Molecular Weight:700.19
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

Chemical Property:

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Technology Process of [BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

There total 1 articles about [BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1522-22-1
1,1,1,5,5,5-hexafluoroacetylacetone

: 603-33-8
triphenylbismuthane

: 1187882-78-5
[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

Guidance literature:: In hexane; hexane was added to BiPh3 in Schlenk flask; stirred and refluxed until dissolved; H2C(C(O)CF3)2 (2 equiv.) was added with stirring within 10 min; refluxed for 30 min; filtered under Ar; concd. (vac.); stored at -20°C overnight; elem. anal.;
DOI:10.1016/j.jorganchem.2009.04.036

Reference yield: 85.0%

: 1187882-78-5
[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 1187882-84-3
[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2(DMSO)]

Guidance literature:: In hexane; dimethyl sulfoxide; soln. of Bi compd. in hexane was treated with DMSO; elem. anal.;
DOI:10.1016/j.jorganchem.2009.04.036

Reference yield: 73.0%

: 1187882-78-5
[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2]

: 100-47-0
benzonitrile

: 1187882-85-4
[BiPh(1,1,1,5,5,5-hexafluoro-2,4-pentanedione)2(PhCN)]

Guidance literature:: In hexane; suspn. of PhCN in hexane was added with stirring to soln. of Bi compd. in hexane; filtered; elem. anal.;
DOI:10.1016/j.jorganchem.2009.04.036