2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Base Information

Chemical Name:2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole
CAS No.:10245-82-6
Molecular Formula:C11H9Br2NO
Molecular Weight:331.007
Hs Code.:
DSSTox Substance ID:DTXSID80454446
Nikkaji Number:J650.233D
Wikidata:Q82275969
Mol file:10245-82-6.mol

Synonyms:2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole;10245-82-6;1H-Pyrrole, 2-(3,5-dibromo-2-methoxyphenyl)-;SCHEMBL8541964;DTXSID80454446;JLXGOYFXOKFPKJ-UHFFFAOYSA-N;2-(3,5-dibromo-2-methoxyphenyl)pyrrole;2-(2-Methoxy-3,5-dibromophenyl)-1H-pyrrole

Suppliers and Price of 2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:330.90304
Heavy Atom Count:15
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)Br)C2=CC=CN2

Technology Process of 2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

There total 13 articles about 2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 121789-40-0
1-(3,5-Dibrom-2-methoxyphenyl)-1,4-butandion

: 10245-82-6
2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Guidance literature:: With ammonium acetate; In acetic acid; for 0.166667h; Ambient temperature;

Reference yield: 42.0%

: 2-(3,5-dibromo-2-methoxyphenyl)-1-(p-tolylsulfonyl)-2,3-dihydro-1H-pyrrole

: 10245-82-6
2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 1.16667h; Inert atmosphere;
DOI:10.1002/ejoc.201402177

Reference yield:

: 61657-65-6
3,5-dibromo-2-methoxybenzaldehyde

: 10245-82-6
2-(3,5-dibromo-2-methoxyphenyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, room temperature, 1 h; 2.) THF, room temperature, 48 h

2: 61 percent / pyridinium dichromate / dimethylformamide / 9 h / Ambient temperature

3: 56 percent / CH₃CO₂NH₄ / acetic acid / Heating

With dipyridinium dichromate; ammonium acetate; magnesium; In acetic acid; N,N-dimethyl-formamide;