dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

Base Information

Chemical Name:dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)
CAS No.:1224509-14-1
Molecular Formula:C₂₉H₃₂ClNPRu*Cl
Molecular Weight:597.53
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

Chemical Property:

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Technology Process of dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

There total 3 articles about dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 140669-65-4
2-(diphenylphosphino)-N-methylaniline

: 1224509-14-1,1224509-19-6
dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

Guidance literature:: In methanol; under Ar; a soln. of Ru-contg. compd. (365E-6 mol) and P-contg. compd. (731E-6 mol) in refluxing methanol (70°C) was stirred for 2 h; the solvent was removed in vac. and residue was dissolved in THF; addn. of diethyl ether; the ppt. was sepd. by filtration and dried in vac.; elem. anal.;
DOI:10.1021/ic100165t

Reference yield:

: dichloro(η6-p-cymene)-(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II), benzene solvate

: 1224509-14-1,1224509-19-6
dichloro(η6-p-cymene)(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

Guidance literature:: In methanol; under Ar; in refluxing methanol at 70°C for 2 h;
DOI:10.1021/ic100165t

Reference yield:

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 140669-65-4
2-(diphenylphosphino)-N-methylaniline

: 1224509-14-1,1224509-19-6
dichloro(η6-p-cymene)-(diphenyl(o-N-methylanilinyl)phosphine)ruthenium(II)

Guidance literature:: In dichloromethane; under Ar; a soln. of Ru-contg. compd. (178E-6 mol) and P-contg. compd. (356E-6 mol) in CH2Cl2 was stirred at ambient temp. (21°C) for 30 min; pptn. with ether;
DOI:10.1021/ic100165t