C₂₄H₃₀F₉NO₅S

Base Information

Chemical Name:C₂₄H₃₀F₉NO₅S
CAS No.:1407187-93-2
Molecular Formula:C₂₄H₃₀F₉NO₅S
Molecular Weight:615.558
Hs Code.:

C<sub>24</sub>H<sub>30</sub>F<sub>9</sub>NO<sub>5</sub>S

Synonyms:

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Chemical Property of C₂₄H₃₀F₉NO₅S

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Technology Process of C₂₄H₃₀F₉NO₅S

There total 3 articles about C₂₄H₃₀F₉NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1407187-91-0
3-(N-dodecyl-2-hydroxyacetamido)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1407187-93-2
C₂₄H₃₀F₉NO₅S

Guidance literature:: 3-(N-dodecyl-2-hydroxyacetamido)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; Inert atmosphere;

With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol302748h

Reference yield:

: 1407187-88-5
3-(dodecylamino)phenyl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1407187-93-2
C₂₄H₃₀F₉NO₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0 - 20 h / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1021/ol302748h

Reference yield:

: 108-46-3
recorcinol

: 1407187-93-2
C₂₄H₃₀F₉NO₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

2.1: palladium diacetate; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; potassium phosphate; toluene / 24 h / 110 °C / Inert atmosphere; Molecular sieve; Microwave irradiation

3.1: triethylamine / dichloromethane / 0 - 20 h / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

With potassium phosphate; 4a,9a-dihydro-9,9-dimethyl-4,5-bis(diphenylphosphino)-xanthene; oxalyl dichloride; palladium diacetate; dimethyl sulfoxide; triethylamine; toluene; In dichloromethane;
DOI:10.1021/ol302748h