N1,N2-Bis[[4-(2-pyridinyl)phenyl]methyl]- 1,2-ethanediamine

Base Information

• Chemical Name: N1,N2-Bis[[4-(2-pyridinyl)phenyl]methyl]- 1,2-ethanediamine
• CAS No.: 1507370-20-8
• Molecular Formula: C₂₆H₂₆N₄
• Molecular Weight: 394.519
• Mol file: 1507370-20-8.mol

Synonyms:

Chemical Property of N1,N2-Bis[[4-(2-pyridinyl)phenyl]methyl]- 1,2-ethanediamine

Chemical Property:

• Boiling Point: 589.9±50.0 °C(Predicted)
• PKA: 9.05±0.20(Predicted)
• Density: 1.125±0.06 g/cm3(Predicted)
• Storage Temp.: 2-8°C
• Solubility.: DMSO: soluble2mg/mL, clear (warmed)

Purity/Quality:

99%+, ^*data from raw suppliers

N1,N2-Bis[4-(2-pyridinyl)benzyl]-1,2-ethanediamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22

MSDS Files:

Useful:

Technology Process of N1,N2-Bis[[4-(2-pyridinyl)phenyl]methyl]- 1,2-ethanediamine

There total 3 articles about N1,N2-Bis[[4-(2-pyridinyl)phenyl]methyl]- 1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(2'-pyridyl)benzaldehyde (127406-56-8) + ethylenediamine (107-15-3,85404-18-8) → C26H26N4 (1507370-20-8)

Guidance literature:

4-(2'-pyridyl)benzaldehyde; ethylenediamine; In ethanol; for 0.5h;

With methanol; sodium tetrahydroborate; for 0.25h; Reflux;

Reference yield:

C26H22N4 → C26H26N4 (1507370-20-8)

Guidance literature:

With methanol; sodium tetrahydroborate; for 0.25h; Reflux;

Reference yield:

4-(2'-pyridyl)benzaldehyde (127406-56-8) → C26H26N4 (1507370-20-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.5 h / Heating

2: sodium tetrahydroborate; methanol / 0.25 h / Reflux

With methanol; sodium tetrahydroborate; In ethanol;

upstream raw materials:

4-(2'-pyridyl)benzaldehyde

ethylenediamine

Refernces

• 1、 -. "FBXO3 INHIBITORS". . . Retrieved 2014/01/08.