C₂₃H₂₈N₂O₆

Base Information

• Chemical Name: C₂₃H₂₈N₂O₆
• CAS No.: 1427682-95-8
• Molecular Formula: C₂₃H₂₈N₂O₆
• Molecular Weight: 428.485
• Mol file: 1427682-95-8.mol

Synonyms:

Chemical Property of C₂₃H₂₈N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₈N₂O₆

There total 9 articles about C₂₃H₂₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

C17H20N2O6 (1427682-85-6) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C23H28N2O6 (1427682-95-8)

Guidance literature:

With ethylenediamine; In methanol; for 5h; Reflux;

DOI:10.3987/COM-12-12611

Reference yield:

C28H26N2O5S (51415-31-7) → C23H28N2O6 (1427682-95-8)

Guidance literature:

Multi-step reaction with 5 steps

1.1: triphenylphosphine; squaric acid / toluene; N,N-dimethyl acetamide / Reflux

2.1: chlorine / tetrachloromethane; ethyl acetate / 20 °C

2.2: 20 °C

3.1: 20 °C

4.1: sodium carbonate / water; acetonitrile / 4 h / 82 °C

5.1: ethylenediamine / methanol / 5 h / Reflux

With chlorine; sodium carbonate; ethylenediamine; triphenylphosphine; squaric acid; In methanol; tetrachloromethane; N,N-dimethyl acetamide; water; ethyl acetate; toluene; acetonitrile;

DOI:10.3987/COM-12-12611

Reference yield:

6-Aminopenicillanic Acid (551-16-6) → C23H28N2O6 (1427682-95-8)

Guidance literature:

Multi-step reaction with 8 steps

1.1: sodium carbonate / water / 0 °C

2.1: peracetic acid / dichloromethane / 0 °C / Reflux

3.1: peracetic acid / dichloromethane / 0 °C

4.1: triphenylphosphine; squaric acid / toluene; N,N-dimethyl acetamide / Reflux

5.1: chlorine / tetrachloromethane; ethyl acetate / 20 °C

5.2: 20 °C

6.1: 20 °C

7.1: sodium carbonate / water; acetonitrile / 4 h / 82 °C

8.1: ethylenediamine / methanol / 5 h / Reflux

With peracetic acid; chlorine; sodium carbonate; ethylenediamine; triphenylphosphine; squaric acid; In methanol; tetrachloromethane; dichloromethane; N,N-dimethyl acetamide; water; ethyl acetate; toluene; acetonitrile;

DOI:10.3987/COM-12-12611

upstream raw materials:

6-Aminopenicillanic Acid

C₂₈H₂₆N₂O₅S

(R)-3-Methyl-2-((1S,5R)-7-oxo-3-phenyl-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-but-3-enoic acid benzhydryl ester

benzoyl chloride