Technology Process of C70H80B2N4S2
There total 4 articles about C70H80B2N4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
LDA;
In
tetrahydrofuran;
(C4H2S(N2(C6H13)C7H5))2Br2 reacted with LDA (4 equiv.) at -78°C, then heated to 0°C, Mes2BF added;
DOI:10.1002/anie.201204050
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(II) acetate monohydrate; caesium carbonate / dimethyl sulfoxide / 96 h / 120 °C / Inert atmosphere
2.1: benzonitrile / 3 h / 150 °C / Inert atmosphere
3.1: lithium diisopropyl amide / tetrahydrofuran / 1.25 h / -78 - 0 °C / Inert atmosphere
3.2: 17 h / -78 - 20 °C / Inert atmosphere
With
copper(II) acetate monohydrate; caesium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide; benzonitrile;
DOI:10.1002/anie.201204050
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(II) acetate monohydrate; caesium carbonate / dimethyl sulfoxide / 96 h / 120 °C / Inert atmosphere
2.1: benzonitrile / 3 h / 150 °C / Inert atmosphere
3.1: lithium diisopropyl amide / tetrahydrofuran / 1.25 h / -78 - 0 °C / Inert atmosphere
3.2: 17 h / -78 - 20 °C / Inert atmosphere
With
copper(II) acetate monohydrate; caesium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; dimethyl sulfoxide; benzonitrile;
DOI:10.1002/anie.201204050
