α,o-bistoluene

Base Information

Chemical Name:α,o-bistoluene
CAS No.:131123-41-6
Molecular Formula:C₁₅H₂₂F₆O₂Si₂
Molecular Weight:404.5
Hs Code.:

α,o-bis<dimethyl(2,2,2-trifluoroethoxy)silyl>toluene

Synonyms:

Suppliers and Price of α,o-bistoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α,o-bistoluene

Chemical Property:

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Technology Process of α,o-bistoluene

There total 3 articles about α,o-bistoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 75-89-8
2,2,2-trifluoroethanol

: 131123-37-0
2,2,3,3-tetramethyl-2,3-disila-1-indanyl chloride

: 138849-85-1
1,1,2,2-tetramethyl-3-(2,2,2-trifluoroethoxy)-1,2-disilaindan

: 131123-41-6
α,o-bistoluene

Guidance literature:: With water; at 25 ℃; Rate constant; solvolysis;
DOI:10.1246/cl.1990.1937

Reference yield:

: 578-51-8
2-bromobenzylchloride

: 131123-41-6
α,o-bistoluene

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / BuLi / hexane; tetrahydrofuran / -100 °C

2: 57 percent / lithiumdiisopropylamide (LDA) / tetrahydrofuran / 2 h / -78 °C

3: 31 percent / 2,6-dimethylpyridine / acetone / 72 h / 25 °C

With 2,6-dimethylpyridine; n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane; acetone;
DOI:10.1246/bcsj.64.3280

Reference yield:

: 138849-94-2
o-(2-chlorotetramethyldisilanyl)benzyl chloride

: 131123-41-6
α,o-bistoluene

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / lithiumdiisopropylamide (LDA) / tetrahydrofuran / 2 h / -78 °C

2: 31 percent / 2,6-dimethylpyridine / acetone / 72 h / 25 °C

With 2,6-dimethylpyridine; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1246/bcsj.64.3280