4-(Dimethylamino)phenylselenium cyanide

Base Information

• Chemical Name: 4-(Dimethylamino)phenylselenium cyanide
• CAS No.: 10272-02-3
• Molecular Formula: C9H10N2Se
• Molecular Weight: 225.152
• Hs Code.: 2929909090
• Mol file: 10272-02-3.mol

Synonyms:N,N-Dimethyl-4-selenocyanato-anilin;(4-dimethylaminophenyl) selenocyanate;Selenocyanic acid,4-(dimethylamino)phenyl ester;4-Dimethylamino-phenylselenocyanat;N,N-Dimethyl-p-selenocyanatoaniline;Selenocyanic acid,p-(dimethylamino)phenyl ester;4-(N,N-Dimethylamino)Phenylselenocyanate;4-dimethylanimophenyl selenocyanate;N,N-dimethyl-4-selenocyanato-aniline;

Chemical Property of 4-(Dimethylamino)phenylselenium cyanide

Chemical Property:

• PSA: 27.03000
• LogP: 0.56318

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(Dimethylamino)phenylselenium cyanide

There total 13 articles about 4-(Dimethylamino)phenylselenium cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-(dimethylamino)benzene-boronic acid (28611-39-4) + potassium selenocyanate (3425-46-5) → 4-(N,N-dimethylamino)phenylselenocyanate (10272-02-3)

Guidance literature:

In water; acetonitrile; at 20 ℃; for 1.33333h; Electrolysis; Green chemistry;

DOI:10.1039/c9gc03797g

Reference yield: 88.0%

potassium selenocyanate (3425-46-5) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → 4-(N,N-dimethylamino)phenylselenocyanate (10272-02-3)

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; In water; at 20 ℃; for 0.5h; Sealed tube; Green chemistry;

DOI:10.1021/acs.joc.0c01035

Reference yield: 63.0%

trimethylsilyl cyanide (7677-24-9) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → 4-(N,N-dimethylamino)phenylselenocyanate (10272-02-3)

Guidance literature:

With selenium; dimethyl sulfoxide; at 120 ℃; for 24h; regioselective reaction;

DOI:10.1039/c8cc07905f

upstream raw materials:

triselenium dicyanide

N,N-dimethyl-aniline

4-chloro-N,N-dimethylaniline

potassium selenocyanate

Downstream raw materials:

N,N-dimethyl-4-[(trifluoromethyl)selanyl]aniline

4,4′(N,N′-dimethylaniline)diselenide