{Et4N}4{Cr4(CO)12(μOPh)4}

Base Information

Chemical Name:{Et4N}4{Cr4(CO)12(μOPh)4}
CAS No.:97879-19-1
Molecular Formula:4C₈H₂₀N*C₃₆H₂₀Cr₄O₁₆
Molecular Weight:1437.54
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {Et4N}4{Cr4(CO)12(μOPh)4}

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Technology Process of {Et4N}4{Cr4(CO)12(μOPh)4}

There total 5 articles about {Et4N}4{Cr4(CO)12(μOPh)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 16800-46-7,22736-49-8
trisacetonitrile(tricarbonyl)chromium⁽⁰⁾

: 32580-85-1
tetraethylammonium phenolate

: 97879-19-1
{Et4N}4{Cr4(CO)12(μOPh)4}

Guidance literature:: In tetrahydrofuran; addn. of solid Et4NOC6H5 to Cr(CO)3(CH3CN)3 in THF, stirred at room temp. for 12h;; filtration, drying in vac., crystn. from THF/CH3CN (85%/15%); elem. anal.;;

Reference yield: 35.0%

: 97879-17-9
4(C₂H₅)4N⁽¹⁺⁾*{Cr₄(CO)12(OH)4}^(4-)={(C₂H₅)4N}4{Cr₄(CO)12(OH)4}

: 32580-85-1
tetraethylammonium phenolate

: 97879-19-1
{Et4N}4{Cr4(CO)12(μOPh)4}

Guidance literature:: In tetrahydrofuran; in refluxing THF;;

Reference yield:

: 15038-41-2
pentacarbonyl(tetrahydrofuran)chromium⁽⁰⁾

: 32580-85-1
tetraethylammonium phenolate

: 97879-19-1
{Et4N}4{Cr4(CO)12(μOPh)4}

Guidance literature:: In tetrahydrofuran; under N2, addn. of a soln. of Cr(CO)5THF to the (Et4N)(OPh), stirring at room temp. overnight; filtration, washing with (CH3)2CO, recrystn. by layering Et2O over a concd. CH3CN soln.;
DOI:10.1021/ja00200a031