C₄₆H₄₈N₄O₁₆

Base Information

Chemical Name:C₄₆H₄₈N₄O₁₆
CAS No.:1287768-46-0
Molecular Formula:C₄₆H₄₈N₄O₁₆
Molecular Weight:912.904
Hs Code.:

C<sub>46</sub>H<sub>48</sub>N<sub>4</sub>O<sub>16</sub>

Synonyms:

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Chemical Property of C₄₆H₄₈N₄O₁₆

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Technology Process of C₄₆H₄₈N₄O₁₆

There total 19 articles about C₄₆H₄₈N₄O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1287768-19-7
C₄₃H₄₆N₄O₁₆

: 70381-98-5
prop-2-yn-1-yl 2,2,2-trichloroacetimidate

: 1287768-46-0
C₄₆H₄₈N₄O₁₆

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; Molecular sieve;
DOI:10.1021/jo200076z

Reference yield:

: 1287768-28-8
phenyl 2,3-di-O-benzoyl-4,6-O-p-methoxy-benzylidene-1-thio-β-D-glucopyranoside

: 1287768-46-0
C₄₆H₄₈N₄O₁₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylsilane; phenylborondichloride / dichloromethane / 0.5 h / -78 °C / Molecular sieve; Inert atmosphere

2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 0 °C

3.2: 1 h / 0 °C

4.1: N-iodo-succinimide; acetic acid / dichloromethane / 20 °C

5.1: trimethylsilylazide; tin(IV) chloride / dichloromethane / 3 h / 20 °C

6.1: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C

7.1: trifluorormethanesulfonic acid / dichloromethane / 20 °C / Molecular sieve

With triethylsilane; N-iodo-succinimide; copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trifluorormethanesulfonic acid; [bis(acetoxy)iodo]benzene; trimethylsilylazide; phenylborondichloride; tin(IV) chloride; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo200076z

Reference yield:

: 1287768-30-2
methyl phenyl 2,3-di-O-benzoyl-4-O-p-methoxybenzyl-1-thio-β-D-glucuronate

: 1287768-46-0
C₄₆H₄₈N₄O₁₆

Guidance literature:: Multi-step reaction with 4 steps

1: N-iodo-succinimide; acetic acid / dichloromethane / 20 °C

2: trimethylsilylazide; tin(IV) chloride / dichloromethane / 3 h / 20 °C

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C

4: trifluorormethanesulfonic acid / dichloromethane / 20 °C / Molecular sieve

With N-iodo-succinimide; copper(l) iodide; trifluorormethanesulfonic acid; trimethylsilylazide; tin(IV) chloride; acetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jo200076z