Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester

Base Information

• Chemical Name: Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester
• CAS No.: 102741-33-3
• Molecular Formula: C9H9ClN2O2
• Molecular Weight: 212.636
• DSSTox Substance ID: DTXSID80358672
• Mol file: 102741-33-3.mol

Synonyms:102741-33-3;Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester;DTXSID80358672

Chemical Property of Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester

Chemical Property:

• XLogP3: 2.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 212.0352552
• Heavy Atom Count: 14
• Complexity: 213

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC(=O)NN=CC1=CC=C(C=C1)Cl

Technology Process of Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester

There total 1 articles about Hydrazinecarboxylic acid, [(4-chlorophenyl)methylene]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrazinecarboxylic acid methyl ester (6294-89-9) + 4-chlorobenzaldehyde (104-88-1) → N'-methoxycarbonyl 4-chlorobenzaldehyde hydrazone (102741-33-3)

Guidance literature:

In methanol;

DOI:10.3184/174751914X14001747558135

Reference yield:

N'-methoxycarbonyl 4-chlorobenzaldehyde hydrazone (102741-33-3) + N'-methoxycarbonyl-N'-propargyl 4-chlorobenzaldehyde hydrazone (139055-31-5) + propargyl bromide (106-96-7) → N'-methoxycarbonyl-N'-3-bromopropargyl 4-chlorobenzaldehyde hydrazone (139055-16-6)

Guidance literature:

With N-Bromosuccinimide; potassium carbonate; silver nitrate; In ethyl acetate; acetone;

Reference yield:

N'-methoxycarbonyl 4-chlorobenzaldehyde hydrazone (102741-33-3) → 5-(4-chlorophenyl)-3-methyl-1,3,4-oxadiazol-2(3H)-one (945-61-9)

Guidance literature:

With iodine; potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 1h;

DOI:10.1039/c5ob02667a

upstream raw materials:

hydrazinecarboxylic acid methyl ester

4-chlorobenzaldehyde

Downstream raw materials:

N'-methoxycarbonyl-N'-3-bromopropargyl 4-chlorobenzaldehyde hydrazone

C₉H₈Cl₂N₂O₂

5-(4-chlorophenyl)-3-methyl-1,3,4-oxadiazol-2(3H)-one

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