Phosphinecarboxylic acid, dichloro-, ethyl ester, oxide

Base Information

• Chemical Name: Phosphinecarboxylic acid, dichloro-, ethyl ester, oxide
• CAS No.: 102831-46-9
• Molecular Formula: C3H5Cl2O3P
• Molecular Weight: 190.951
• Mol file: 102831-46-9.mol

Synonyms:ethoxycarbonyl phosphonic dichloride;(ethoxycarbonyl)phosphonic dichloride;ethoxycarbonyl phosphodichloridate;carbethoxyphosphodichloridate;ethyl (dichlorophosphonyl)formate;(ethoxycarbonyl)phosphoric dichloride;

Chemical Property of Phosphinecarboxylic acid, dichloro-, ethyl ester, oxide

Chemical Property:

• Boiling Point: 84 - 86 °C (10 mmHg)
• PSA: 53.18000
• LogP: 2.81360

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphinecarboxylic acid, dichloro-, ethyl ester, oxide

There total 1 articles about Phosphinecarboxylic acid, dichloro-, ethyl ester, oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.5%

bis(trimethylsilyl)(ethoxycarbonyl)phosphonate (66191-00-2) → chloro-trimethyl-silane (75-77-4) + (ethoxycarbonyl)phosphinic dichloride (102831-46-9)

Guidance literature:

With thionyl chloride; for 4h; Heating;

DOI:10.1021/jm00158a012

Reference yield: 44.0%

2,6-diisopropylphenol (2078-54-8) + (ethoxycarbonyl)phosphinic dichloride (102831-46-9) + alanine isopropyl ester hydrochloride (39613-92-8,62062-56-0,62062-65-1) → isopropyl (S)-2-[[(2,6-diisopropylphenoxy)(ethoxycarbonyl)phosphoryl]amino]propanoate

Guidance literature:

With triethylamine; In dichloromethane; at -20 - 20 ℃; for 2h;

upstream raw materials:

bis(trimethylsilyl)(ethoxycarbonyl)phosphonate

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