Technology Process of Allyl 2,6-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-galactopyranoside
There total 6 articles about Allyl 2,6-di-O-benzyl-3-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-α-D-galactopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
calcium hydride; iodine; silver carbonate;
In
toluene;
Ambient temperature;
a) 20 min, b) 48 h;
DOI:10.1016/0008-6215(93)84222-R
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 30.7 percent / Dowex-50 X-8 (H(1+)) / 17.5 h / Heating
2: 81.2 percent / p-toluenesulfonic acid, 4A molecular sieves / 1.5 h / Heating
3: 97 percent / NaH / dimethylformamide / 3 h
4: 86.5 percent / 1N HCl / methanol
5: 52 percent / a) CaH2, b) Ag2CO3, I2 / toluene / Ambient temperature; a) 20 min, b) 48 h
With
hydrogenchloride; calcium hydride; 4 A molecular sieve; Dowex-50 X-8 (H(1+)); iodine; sodium hydride; toluene-4-sulfonic acid; silver carbonate;
In
methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(93)84222-R
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97 percent / NaH / dimethylformamide / 3 h
2: 86.5 percent / 1N HCl / methanol
3: 52 percent / a) CaH2, b) Ag2CO3, I2 / toluene / Ambient temperature; a) 20 min, b) 48 h
With
hydrogenchloride; calcium hydride; iodine; sodium hydride; silver carbonate;
In
methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0008-6215(93)84222-R
