tris-(2-<3--propanamido>ethyl)amine

Base Information

Chemical Name:tris-(2-<3--propanamido>ethyl)amine
CAS No.:136413-30-4
Molecular Formula:C₆₀H₉₀N₁₀O₁₅
Molecular Weight:1191.43
Hs Code.:

tris-(2-<3-<N-benzyloxy-3-(t-butoxycarbonylamino)propanamido>-propanamido>ethyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris-(2-<3--propanamido>ethyl)amine

Chemical Property:

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Technology Process of tris-(2-<3--propanamido>ethyl)amine

There total 6 articles about tris-(2-<3--propanamido>ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 4097-89-6
2,2',2''-triaminotriethylamine

: 136413-26-8
3-[Benzyloxy-(3-tert-butoxycarbonylamino-propionyl)-amino]-propionic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 136413-30-4
tris-(2-<3--propanamido>ethyl)amine

Guidance literature:: In N,N-dimethyl-formamide; at 38 ℃; for 40h;

Reference yield:

: 622-33-3
N-benzyloxyamine

: 136413-30-4
tris-(2-<3--propanamido>ethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / Et₃N, isobutyl chloroformate / tetrahydrofuran / 1.) -15 deg C, 3 h, 2.) r.t., 20 h

2: 80 percent / 60percent NaH / dimethylformamide / 3 h / 100 °C

3: 93 percent / NaOH / methanol / 1.5 h / Ambient temperature

4: 100 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDC*HCl) / Ambient temperature

5: 73 percent / dimethylformamide / 40 h / 38 °C

With sodium hydroxide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; isobutyl chloroformate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

Reference yield:

: 3303-84-2
3-(tert-butyloxycarbonylamino)propionic acid

: 136413-30-4
tris-(2-<3--propanamido>ethyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / Et₃N, isobutyl chloroformate / tetrahydrofuran / 1.) -15 deg C, 3 h, 2.) r.t., 20 h

2: 80 percent / 60percent NaH / dimethylformamide / 3 h / 100 °C

3: 93 percent / NaOH / methanol / 1.5 h / Ambient temperature

4: 100 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (EDC*HCl) / Ambient temperature

5: 73 percent / dimethylformamide / 40 h / 38 °C

With sodium hydroxide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; isobutyl chloroformate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;