2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone

Base Information

• Chemical Name: 2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone
• CAS No.: 1299468-29-3
• Molecular Formula: C₁₈H₂₂N₂O₂
• Molecular Weight: 298.385
• Mol file: 1299468-29-3.mol

Synonyms:

Chemical Property of 2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone

There total 1 articles about 2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-(2,4-dimethoxyphenyl)-2-methylpropan-1-one (86774-65-4) + phenylhydrazine (100-63-0) → 2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone (1299468-29-3)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; Reflux;

DOI:10.1016/j.jphotochem.2010.09.006

Reference yield: 67.0%

2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone (1299468-29-3) → 2-(2,4-dimethoxyphenyl)-3,3-dimethyl-3H-indole (1299468-25-9)

Guidance literature:

With boron trifluoride diethyl etherate; for 4h; Reflux;

DOI:10.1016/j.jphotochem.2010.09.006

Reference yield: 65.0%

2,4-dimethoxyphenyl isopropyl ketone phenylhydrazone (1299468-29-3) → 2-(2-hydroxy-4-methoxyphenyl)-3,3-dimethyl-3H-indole (1299468-28-2)

Guidance literature:

With acetic acid; for 48h; Reflux;

DOI:10.1016/j.jphotochem.2010.09.006

upstream raw materials:

1-(2,4-dimethoxyphenyl)-2-methylpropan-1-one

phenylhydrazine

Downstream raw materials:

2-(2-hydroxy-4-methoxyphenyl)-3,3-dimethyl-3H-indole

2-(2,4-dimethoxyphenyl)-3,3-dimethyl-3H-indole