Technology Process of C25H34N2O
There total 6 articles about C25H34N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium acetate; sodium tris(acetoxy)borohydride;
In
dichloromethane;
at 20 ℃;
for 15h;
Cooling with ice;
DOI:10.1248/cpb.59.1376
- Guidance literature:
-
Multi-step reaction with 6 steps
1: tetrahydrofuran; diethyl ether / 2 h / -20 - 0 °C
2: sulfuric acid / acetic acid / 4 h / 20 °C / Cooling with ice
3: acetic acid; thiourea / ethanol / 16 h / Reflux
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 72 h / 20 °C / Cooling with ice
5: hydrogenchloride / water; ethyl acetate / 2 h / 20 °C / Cooling with ice
6: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 15 h / 20 °C / Cooling with ice
With
hydrogenchloride; sulfuric acid; sodium acetate; sodium tris(acetoxy)borohydride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; thiourea;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; acetic acid; ethyl acetate; acetonitrile;
2: Ritter reaction;
DOI:10.1248/cpb.59.1376
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; ethyl acetate / 2 h / 20 °C / Cooling with ice
2: sodium acetate; sodium tris(acetoxy)borohydride / dichloromethane / 15 h / 20 °C / Cooling with ice
With
hydrogenchloride; sodium acetate; sodium tris(acetoxy)borohydride;
In
dichloromethane; water; ethyl acetate;
DOI:10.1248/cpb.59.1376