bromo{2-(phenylazo)phenyl methyl thioether-N⁽²⁾,S}{2-(phenylazo)phenyl methyl thioether-C⁽⁸⁾,N⁽²⁾,S}ruthenium(II)

Base Information

• Chemical Name: bromo{2-(phenylazo)phenyl methyl thioether-N⁽²⁾,S}{2-(phenylazo)phenyl methyl thioether-C⁽⁸⁾,N⁽²⁾,S}ruthenium(II)
• CAS No.: 101377-22-4
• Molecular Formula: C₂₆H₂₃BrN₄RuS₂
• Molecular Weight: 636.601

Synonyms:

Chemical Property of bromo{2-(phenylazo)phenyl methyl thioether-N⁽²⁾,S}{2-(phenylazo)phenyl methyl thioether-C⁽⁸⁾,N⁽²⁾,S}ruthenium(II)

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Technology Process of bromo{2-(phenylazo)phenyl methyl thioether-N⁽²⁾,S}{2-(phenylazo)phenyl methyl thioether-C⁽⁸⁾,N⁽²⁾,S}ruthenium(II)

There total 1 articles about bromo{2-(phenylazo)phenyl methyl thioether-N⁽²⁾,S}{2-(phenylazo)phenyl methyl thioether-C⁽⁸⁾,N⁽²⁾,S}ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

ruthenium(III) chloride trihydrate (14898-67-0) + 2-(methylthio)azobenzene (101418-85-3) + lithium bromide (7550-35-8) → bis{2-(phenylazo)phenyl methyl thioether-C(8),N(2),S}ruthenium(II) (101377-16-6) + bromo{2-(phenylazo)phenyl methyl thioether-N(2),S}{2-(phenylazo)phenyl methyl thioether-C(8),N(2),S}ruthenium(II) (101377-22-4)

Guidance literature:

In methanol; N2 passed for 5min through a warmed soln. of thioether; LiBr added immediately after addn. of RuCl3*3H2O; heated to reflux for 4 h; evapd.; cooled to room temp.; filtered; washed (H2O, diethyl ether); dried (vac., over P4O10); dissolved (CH2Cl2); chromd. (silica gel); eluted (benzene) (1st product); eluted (CH2Cl2); evapd.; ground with acetonitrile; filtered; crystd. from CH2Cl2/heptane (1:3); elem.anal.;

upstream raw materials:

ruthenium(III) chloride trihydrate

2-(methylthio)azobenzene

lithium bromide

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