tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-)

Base Information

• Chemical Name: tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-)
• CAS No.: 96055-94-6
• Molecular Formula: C₄H₁₂N*C₉H₁₄B₉INS
• Molecular Weight: 466.632

Synonyms:

Chemical Property of tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-)

Chemical Property:

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Technology Process of tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-)

There total 2 articles about tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

Na(1+)*SCNC6H4C2B9H11(1-) + chloroamine-T (127-65-1) + tetramethlyammonium chloride (75-57-0) → tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate(1-) (96055-94-6)

Guidance literature:

With NaI; In water; reagents were dissolved in 0.05 M phosphate buffer and mixed with stirring; after 5 min product was pptd. with excess aq. Me4NCl and washed with water, ppt. was recrystd. from acetone/water; elem.anal.;

DOI:10.1021/ic00206a043

Reference yield: 52.0%

tetramethylammonium 7-(p-isothiocyanatophenyl)dodecahydro-7,8-dicarba-nido-undecaborate(1-) (96095-21-5) + tetramethlyammonium chloride (75-57-0) → tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate(1-) (96055-94-6)

Guidance literature:

With I₂; In ethanol; under N2, mixt. of reagents were stirred overnight at room temp.; soln. was filtered, solvent was removed, residue was dissolved in waterand product was pptd. by addition of excess aq. Me4NCl, ppt. was washedwith water, recrystd. from acetone/water; elem.anal.;

DOI:10.1021/ic00206a043

Reference yield:

tetramethylammonium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate(1-) (96055-94-6) → sodium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate(1-) (96055-95-7)

Guidance literature:

product was obtained by sodium cation exchange;

DOI:10.1021/ic00206a043

upstream raw materials:

tetramethylammonium 7-(p-isothiocyanatophenyl)dodecahydro-7,8-dicarba-nido-undecaborate^(1-)

tetramethlyammonium chloride

chloroamine-T

Downstream raw materials:

sodium 7-(p-isothiocyanatophenyl)-9-iodododecahydro-7,8-dicarba-nido-undecaborate^(1-)

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