1,1-dimethyl-2-benzoylhydrazide hydrochloride

Base Information

• Chemical Name: 1,1-dimethyl-2-benzoylhydrazide hydrochloride
• CAS No.: 1444-57-1
• Molecular Formula: C₉H₁₂N₂O*ClH
• Molecular Weight: 200.668
• Mol file: 1444-57-1.mol

Synonyms:

Chemical Property of 1,1-dimethyl-2-benzoylhydrazide hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-dimethyl-2-benzoylhydrazide hydrochloride

There total 2 articles about 1,1-dimethyl-2-benzoylhydrazide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N',N'-dimethyl-N-vinylbenzohydrazide (249760-03-0) → 1,1-dimethyl-2-benzoylhydrazide hydrochloride (1444-57-1)

Guidance literature:

With hydrogenchloride; In tetrachloromethane;

DOI:10.1023/A:1021643510974

Reference yield:

oxalyl dichloride (79-37-8) + 1-benzoyl-2,2-dimethylhydrazine (1128-86-5) → 3-methyl-5-phenyl-1,3,4-oxadiazol-2(3H)-one (879-60-7) + 1,1-dimethyl-2-benzoylhydrazide hydrochloride (1444-57-1)

Guidance literature:

In chloroform-d1; at 25 - 40 ℃; for 5h; Yield given. Yields of byproduct given;

upstream raw materials:

oxalyl dichloride

1-benzoyl-2,2-dimethylhydrazine

N',N'-dimethyl-N-vinylbenzohydrazide