1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane

Base Information

• Chemical Name: 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane
• CAS No.: 100116-95-8
• Molecular Formula: C₁₂H₁₄Cl₂
• Molecular Weight: 229.149

Synonyms:

Chemical Property of 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane

Chemical Property:

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Technology Process of 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane

There total 1 articles about 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloroform (67-66-3,8013-54-5) + p-methyl-β,β-dimethylstyrene (5916-22-3) → 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane (100116-95-8)

Guidance literature:

With potassium tert-butylate; In Petroleum ether;

Reference yield:

cyclopentadienyl iron(II) dicarbonyl dimer (38117-54-3) + 1,1-dichloro-2,2-dimethyl-3-p-tolylcyclopropane (100116-95-8) + tetra(n-butyl)ammonium hydrogensulfate (32503-27-8) → C5H5Fe(CO)(CO)(CC(C6H4CH3)(CH(CH3)2))Fe(CO)C5H5

Guidance literature:

In tetrahydrofuran; sodium hydroxide; aq. NaOH; 50:50 NaOH:H2O, phase-transfer conditions;

DOI:10.1021/ja00406a045

upstream raw materials:

chloroform

p-methyl-β,β-dimethylstyrene

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