C₉H₁₃NOS

Base Information

• Chemical Name: C₉H₁₃NOS
• CAS No.: 121034-20-6
• Molecular Formula: C₉H₁₃NOS
• Molecular Weight: 183.274

Synonyms:

Chemical Property of C₉H₁₃NOS

Chemical Property:

Purity/Quality:

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Technology Process of C₉H₁₃NOS

There total 1 articles about C₉H₁₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3-methylphenyl sulphide (34786-24-8) → C9H13NOS (121034-20-6,121034-22-8)

Guidance literature:

With [bis(acetoxy)iodo]benzene; ammonium carbamate; In methanol; at 25 ℃; for 3h;

DOI:10.1002/asia.201800889

Reference yield:

C9H13NOS (121034-20-6,121034-22-8) + methyl iodide (74-88-4) → C10H15NOS

Guidance literature:

C₉H₁₃NOS; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 20 ℃;

DOI:10.1002/asia.201800889

Reference yield:

C9H13NOS (121034-20-6,121034-22-8) → C21H35NOSSi

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

1.2: 20 °C

2.1: silver carbonate; tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate / 1,2-dichloro-ethane / 12 h / 90 °C / Sealed tube

With tris(acetonitrile)(η5-pentamethylcyclopentadienyl)rhodium(III) hexafluoroantimonate; sodium hydride; silver carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;

DOI:10.1002/asia.201800889

upstream raw materials:

ethyl 3-methylphenyl sulphide

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