3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

Base Information

Chemical Name:3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil
CAS No.:778603-72-8
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:

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Chemical Property of 3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

Chemical Property:

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Technology Process of 3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

There total 6 articles about 3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4028-66-4
2,4,6-trimethylanisole

: 778603-72-8
3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

Guidance literature:: Multi-step reaction with 4 steps

1: tetrachloromethane; bromine / 10 - 15 °C

2: magnesium; diethyl ether / anschliessend Behandeln mit festem Kohlendioxid bei -5grad

3: thionyl chloride

4: benzene; magnesium; MgI₂ / Reagens 4: Aether

With tetrachloromethane; thionyl chloride; diethyl ether; bromine; magnesium; magnesium iodide; benzene;
DOI:10.1021/ja01855a034

Reference yield:

: 118042-66-3
1-Bromo-3-methoxy-2,4,6-trimethylbenzene

: 778603-72-8
3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium; diethyl ether / anschliessend Behandeln mit festem Kohlendioxid bei -5grad

2: thionyl chloride

3: benzene; magnesium; MgI₂ / Reagens 4: Aether

With thionyl chloride; diethyl ether; magnesium; magnesium iodide; benzene;
DOI:10.1021/ja01855a034

Reference yield:

: 318294-42-7
3-methoxy-2,4,6-trimethylbenzoic acid

: 778603-72-8
3,3'-Dimethoxy-2,4,6,2',4',6'-hexamethyl-benzil

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: benzene; magnesium; MgI₂ / Reagens 4: Aether

With thionyl chloride; magnesium; magnesium iodide; benzene;
DOI:10.1021/ja01855a034