Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester

Base Information

• Chemical Name: Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester
• CAS No.: 68428-00-2
• Molecular Formula: C₃₂H₄₈Cl₂O₃
• Molecular Weight: 551.637
• Mol file: 68428-00-2.mol

Synonyms:

Chemical Property of Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester

There total 5 articles about Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dichloronitrobenzene (99-54-7) → Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester (68428-00-2)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: ammonium hydroxide; hydrogen sulfide / ethanol / Heating

3: (i) NaNO₂, aq. HCl, (ii) CuCl, aq. HCl

4: pyridine / chloroform

With pyridine; ammonium hydroxide; hydrogen sulfide; potassium carbonate; In ethanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

2-(2'-Chloro-4'-aminophenyl)-5,5-dimethyl-1,3-cyclohexanedione (68427-39-4) → Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester (68428-00-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) NaNO₂, aq. HCl, (ii) CuCl, aq. HCl

2: pyridine / chloroform

With pyridine; In chloroform;

Reference yield:

2-(2'-Chloro-4'-nitrophenyl)-5,5-dimethyl-1,3-cyclohexanedione (68427-38-3) → Octadecanoic acid 2-(2,4-dichloro-phenyl)-5,5-dimethyl-3-oxo-cyclohex-1-enyl ester (68428-00-2)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium hydroxide; hydrogen sulfide / ethanol / Heating

2: (i) NaNO₂, aq. HCl, (ii) CuCl, aq. HCl

3: pyridine / chloroform

With pyridine; ammonium hydroxide; hydrogen sulfide; In ethanol; chloroform;

upstream raw materials:

2-(2',4'-Dichlorophenyl)-5,5-dimethyl-1,3-cyclohexanedione

Stearoyl chloride

3,4-dichloronitrobenzene

2-(2'-Chloro-4'-aminophenyl)-5,5-dimethyl-1,3-cyclohexanedione