(R)-4'-(1-hydroxy-ethyl)benzoic methyl ester

Base Information

Chemical Name:(R)-4'-(1-hydroxy-ethyl)benzoic methyl ester
CAS No.:129446-47-5
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:

Synonyms:

Suppliers and Price of (R)-4'-(1-hydroxy-ethyl)benzoic methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of (R)-4'-(1-hydroxy-ethyl)benzoic methyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of (R)-4'-(1-hydroxy-ethyl)benzoic methyl ester

There total 19 articles about (R)-4'-(1-hydroxy-ethyl)benzoic methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67-56-1
methanol

: 124-38-9,18923-20-1
carbon dioxide

: 5391-88-8,25675-29-0,76155-78-7,100760-04-1
(S)-1-(4-bromophenyl)ethanol

: 79322-76-2,84851-56-9,129446-47-5,102681-71-0
methyl 4-[(1S)-1-hydroxyethyl]benzoate

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine; In acetonitrile; at 100 ℃; for 6h; under 5168.02 Torr; Autoclave;

Reference yield: 98.0%

: 3609-53-8
methyl 4-acetylbenzoate

: 79322-76-2,84851-56-9,102681-71-0,129446-47-5
(R)-4'-(1-hydroxy-ethyl)benzoic methyl ester

Guidance literature:: methyl 4-acetylbenzoate; With Triethoxysilane; (S,E)-(+)-2,6-diisopropyl-N-(2-((2-(4-phenyl-4,5-dihydrooxazol-2-yl)phenyl)amino)benzylidene)aniline; sodium triethylborohydride; cobalt(II) chloride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 15h; Schlenk technique; Inert atmosphere;

With potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; at 20 ℃; for 2h; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02260

Reference yield: 95.0%

: 3609-53-8
methyl 4-acetylbenzoate

: 79322-76-2,84851-56-9,129446-47-5,102681-71-0
methyl 4-[(1S)-1-hydroxyethyl]benzoate

Guidance literature:: methyl 4-acetylbenzoate; With diethoxymethylane; C₃₆H₃₁FeN₃O₃; In toluene; at -78 - 20 ℃; for 6h; Schlenk technique; Inert atmosphere;

With potassium carbonate; In methanol; at 20 ℃; for 1h; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja512986m