2,7,12,17,22-Pentaazahexacosanedioic acid, 23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-, 26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Base Information

Chemical Name:2,7,12,17,22-Pentaazahexacosanedioic acid, 23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-, 26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-
CAS No.:103346-43-6
Molecular Formula:C37H59N5O10
Molecular Weight:733.903
Hs Code.:

2,7,12,17,22-Pentaazahexacosanedioic acid,
23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-,
26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Synonyms:

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Chemical Property of 2,7,12,17,22-Pentaazahexacosanedioic acid, 23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-, 26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2,7,12,17,22-Pentaazahexacosanedioic acid, 23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-, 26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)-

There total 7 articles about 2,7,12,17,22-Pentaazahexacosanedioic acid, 23-[(1,1-dimethylethoxy)carbonyl]-6,11,16,21-tetraoxo-, 26-(1,1-dimethylethyl) 1-(phenylmethyl) ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 32677-01-3
L-glutamic acid di-tert-butyl ester hydrochloride

: 103321-33-1
4-{4-[4-(4-Benzyloxycarbonylamino-butyrylamino)-butyrylamino]-butyrylamino}-butyric acid

: 103346-43-6
(S)-2-(4-{4-[4-(4-Benzyloxycarbonylamino-butyrylamino)-butyrylamino]-butyrylamino}-butyrylamino)-pentanedioic acid di-tert-butyl ester

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1021/jm00160a014

Reference yield:

: 5105-78-2
4-(benzyloxycarbonylamino)butyric acid

: 103346-43-6
(S)-2-(4-{4-[4-(4-Benzyloxycarbonylamino-butyrylamino)-butyrylamino]-butyrylamino}-butyrylamino)-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: Et₃N / dimethylformamide / 0.33 h

2: Et₃N / dimethylformamide / 0.5 h

3: 97 percent / Ba(OH)2.8H₂O / ethanol; H₂O / Ambient temperature

4: Et₃N / dimethylformamide / 0.33 h

5: Et₃N / dimethylformamide / 0.5 h

6: 97 percent / Ba(OH)2.8H₂O / ethanol; H₂O / Ambient temperature

7: 100 percent / diphenylphosphoryl azide (DPPA), Et₃N / dimethylformamide / Ambient temperature

With barium dihydroxide; diphenylphosphoranyl azide; triethylamine; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00160a014

Reference yield:

: 1489-76-5
4-(4-Benzyloxycarbonylamino-butyrylamino)-butyric acid

: 103346-43-6
(S)-2-(4-{4-[4-(4-Benzyloxycarbonylamino-butyrylamino)-butyrylamino]-butyrylamino}-butyrylamino)-pentanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / dimethylformamide / 0.33 h

2: Et₃N / dimethylformamide / 0.5 h

3: 97 percent / Ba(OH)2.8H₂O / ethanol; H₂O / Ambient temperature

4: 100 percent / diphenylphosphoryl azide (DPPA), Et₃N / dimethylformamide / Ambient temperature

With barium dihydroxide; diphenylphosphoranyl azide; triethylamine; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00160a014