N,N-Dimethyl-4-(4-nitrophenylazo)-1-naphthylamine

Base Information

• Chemical Name: N,N-Dimethyl-4-(4-nitrophenylazo)-1-naphthylamine
• CAS No.: 10336-21-7
• Molecular Formula: C₁₈H₁₆N₄O₂
• Molecular Weight: 320.351
• Hs Code.: 2927000090
• European Community (EC) Number: 634-411-7
• DSSTox Substance ID: DTXSID60394977
• Nikkaji Number: J1.077.295H
• Mol file: 10336-21-7.mol

Synonyms:10336-21-7;N,N-dimethyl-4-[(4-nitrophenyl)diazenyl]naphthalen-1-amine;1-Naphthalenamine, N,N-dimethyl-4-[(4-nitrophenyl)azo]-;N,N-DIMETHYL-4-(4-NITROPHENYLAZO)-1-NAPHTHYLAMINE;1-(4-nitro-phenylazo)-4-(dimethylamino)naphtalene;N,N-DiMethyl-4-[(E)-(4-nitrophenyl)diazenyl]-1-naphthalenaMine;SCHEMBL5044863;DTXSID60394977;TYDHNGUGPAPPNO-UHFFFAOYSA-N;AKOS024339706;4-(4-Nitrophenylazo)-N,N-dimethyl-1-naphthalenamine

Chemical Property of N,N-Dimethyl-4-(4-nitrophenylazo)-1-naphthylamine

Chemical Property:

• PSA: 73.78000
• LogP: 5.75260
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 320.12732577
• Heavy Atom Count: 24
• Complexity: 454

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C2=CC=CC=C21)N=NC3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of N,N-Dimethyl-4-(4-nitrophenylazo)-1-naphthylamine

There total 2 articles about N,N-Dimethyl-4-(4-nitrophenylazo)-1-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-1-naphthalenamine (86-56-6,112790-02-0,651316-60-8) + 4-nitro-aniline (100-01-6,104810-17-5) → dimethyl-[4-(4-nitro-phenylazo)-[1]naphthyl]-amine (10336-21-7)

Guidance literature:

4-nitro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 4 ℃; for 0.25h;

N,N-dimethyl-1-naphthalenamine; With potassium acetate; In water; acetic acid; at 20 ℃; for 1.5h; Cooling with ice;

Reference yield:

N,N-dimethyl-1-naphthalenamine (86-56-6,112790-02-0,651316-60-8) + 4-nitrobenzenediazonium chloride (100-05-0) → dimethyl-[4-(4-nitro-phenylazo)-[1]naphthyl]-amine (10336-21-7)

Guidance literature:

Reference yield:

dimethyl-[4-(4-nitro-phenylazo)-[1]naphthyl]-amine (10336-21-7) → 1-(4-amino-phenylazo)-4-(dimethylamino)naphtalene (79779-19-4)

Guidance literature:

With sodium hydrogen sulfate; In methanol; water; for 3h; Heating / reflux;

upstream raw materials:

N,N-dimethyl-1-naphthalenamine

4-nitrobenzenediazonium chloride

4-nitro-aniline

Downstream raw materials:

1-(4-amino-phenylazo)-4-(dimethylamino)naphtalene