α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

Base Information

Chemical Name:α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle
CAS No.:63741-26-4
Molecular Formula:C₂₁H₃₄O₄S
Molecular Weight:382.565
Hs Code.:

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Chemical Property of α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

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Technology Process of α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

There total 4 articles about α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-13-0
Octanal

: 58059-08-8
tert-butyl (R)-p-toluenesulfinylacetate

: 63741-26-4
α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

Guidance literature:: With tert-butylmagnesium bromide; In tetrahydrofuran; at -78 ℃; Yield given;
DOI:10.1016/0040-4020(80)80010-X

Reference yield:

: 540-88-5
acetic acid tert-butyl ester

: 63741-26-4
α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

Guidance literature:: Multi-step reaction with 2 steps

1: 1) (iPr)2NMgBr; 2) NH₄Cl / 1) THF, ether, -40 to -35 deg C

2: t-BuMgBr / tetrahydrofuran / -78 °C

With bromomagnesium diisopropylamide; tert-butylmagnesium bromide; ammonium chloride; In tetrahydrofuran;
DOI:10.1016/0040-4020(80)80010-X

Reference yield:

: 824-79-3
sodium 4-methylbenzenesulfinate

: 63741-26-4
α-(p-tolylsulfinyl) β-hydroxy n-decanoate de t-butyle

Guidance literature:: Multi-step reaction with 3 steps

1: 1) thyonyl chloride / 1) 1 h, 0 deg C; 2) ether, pyridine, 2 h, RT

2: 1) (iPr)2NMgBr; 2) NH₄Cl / 1) THF, ether, -40 to -35 deg C

3: t-BuMgBr / tetrahydrofuran / -78 °C

With thionyl chloride; bromomagnesium diisopropylamide; tert-butylmagnesium bromide; ammonium chloride; In tetrahydrofuran;
DOI:10.1016/0040-4020(80)80010-X