4-Hydroxy-6-nitro-quinoline-3-carboxylic acid ethyl ester

Base Information

• Chemical Name: 4-Hydroxy-6-nitro-quinoline-3-carboxylic acid ethyl ester
• CAS No.: 103514-53-0
• Molecular Formula: C12H10N2O5
• Molecular Weight: 262.21800
• Hs Code.: 2933499090
• Mol file: 103514-53-0.mol

Synonyms:ethyl 4-hydroxy-6-nitroquinoline-3-carboxylate;3-quinolinecarboxylic acid,4-hydroxy-6-nitro-,ethyl ester;ethyl 6-nitro-4-oxo-1,4-dihydroquinoline-3-carboxylate;

Chemical Property of 4-Hydroxy-6-nitro-quinoline-3-carboxylic acid ethyl ester

Chemical Property:

• PSA: 104.98000
• LogP: 2.13620

Purity/Quality:

99% ^*data from raw suppliers

Ethyl4-Hydroxy-6-nitroquinoline-3-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Hydroxy-6-nitro-quinoline-3-carboxylic acid ethyl ester

There total 10 articles about 4-Hydroxy-6-nitro-quinoline-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethyl α-ethoxycarbonyl-β-(4-nitroanilino)acrylate (78596-42-6) → ethyl 6-nitro-4-oxo-1,4-dihydroquinoline-3-carboxylate (103514-53-0,175087-43-1)

Guidance literature:

In diphenylether; for 1h; Reflux;

DOI:10.5560/ZNB.2013-3009

Reference yield: 80.0%

4-nitro-aniline (100-01-6,104810-17-5) + diethyl 2-ethoxymethylenemalonate (87-13-8) → ethyl 6-nitro-4-oxo-1,4-dihydroquinoline-3-carboxylate (103514-53-0,175087-43-1)

Guidance literature:

for 0.0333333h; Irradiation;

Reference yield: 30.0%

ethyl α-ethoxycarbonyl-β-(4-nitroanilino)acrylate (78596-42-6) → 6-nitro-4-hydroxy-quinoline-3-carboxylic acid ethylester (103514-53-0)

Guidance literature:

With Dowtherm A; for 1h; Heating / reflux;

upstream raw materials:

diphenylether

biphenyl

ethyl α-ethoxycarbonyl-β-(4-nitroanilino)acrylate

4-nitro-aniline

Downstream raw materials:

6-nitro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid

Ethyl 4-chloro-6-nitro-quinoline-3-carboxylate

6-nitroquinoline-4(1H)-one

4-chloro-6-nitroquinoline

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